INSTRUMENT CONTROL PARAMETERS: 29DD -------------------------------------- C:\MSDCHEM\1\METHODS\CRATTRAY\8270_splitless_275.M Fri Nov 11 15:44:15 2011 Control Information ------- ----------- Sample Inlet : GC Injection Source : GC ALS Mass Spectrometer : Enabled Oven Equilibration Time 0.5 min Oven Program On 40 蚓 for 1 min then 25 蚓/min to 280 蚓 for 0 min then 5 蚓/min to 320 蚓 for 1 min Run Time 19.6 min Front Injector Syringe Size 10 無 Injection Volume 1 無 Injection Repetitions 1 Injection Delay 0 sec Solvent A Washes (PreInj) 3 Solvent A Washes (PostInj) 3 Solvent A Volume 8 無 Solvent B Washes (PreInj) 0 Solvent B Washes (PostInj) 0 Solvent B Volume 8 無 Sample Washes 1 Sample Wash Volume 3 無 Sample Pumps 5 Dwell Time (PreInj) 0 min Dwell Time (PostInj) 0 min Solvent Wash Draw Speed 300 無/min Solvent Wash Dispense Speed 6000 無/min Sample Wash Draw Speed 300 無/min Sample Wash Dispense Speed 6000 無/min Injection Dispense Speed 6000 無/min Viscosity Delay 0 sec Sample Depth Disabled Sample Overlap Sample overlap is not enabled Front SS Inlet He Mode Pulsed Splitless Heater On 270 蚓 Pressure On 9.1473 psi Total Flow On 104.03 mL/min Septum Purge Flow On 3 mL/min Gas Saver On 20 mL/min After 3 min Injection Pulse Pressure 30 psi Until 0.64 min Purge Flow to Split Vent 100 mL/min at 0.59 min Back SS Inlet He Mode Split Heater Off Pressure Off Total Flow Off Septum Purge Flow Off Gas Saver On 20 mL/min After 2 min Split Ratio 100 :1 Split Flow 0 mL/min Thermal Aux 2 {MSD Transfer Line} Heater On Temperature Program On 280 蚓 for 0 min Run Time 19.6 min Column #1 Rxi-5silMSRxi-5silMS 350 蚓: 30 m x 250 痠 x 0.25 痠 In: Front SS Inlet He Out: Vacuum (Initial) 40 蚓 Pressure 9.1473 psi Flow 1.2 mL/min Average Velocity 39.723 cm/sec Holdup Time 1.2587 min Flow Program On 1.2 mL/min for 5 min Run Time 19.6 min Column #2 Rxi-624Sil MSRxi-624Sil MS 340 蚓: 30 m x 250 痠 x 1.4 痠 In: Front SS Inlet He Out: Other (Initial) 40 蚓 Pressure 15.375 psi Flow 1.2 mL/min Average Velocity 27.649 cm/sec Holdup Time 1.8084 min Flow Program Off 1.2 mL/min for 0 min Run Time 19.6 min Column #3 Rxi-5Sil MS with 5m integraguaRxi-5Sil MS with 5m integragua 350 蚓: 35 m x 250 痠 x 0.25 痠 In: Front SS Inlet He Out: Vacuum (Initial) 40 蚓 Pressure 9.1473 psi Flow 1.0286 mL/min Average Velocity 34.048 cm/sec Holdup Time 1.7133 min Pressure Program On 9.1473 psi for 0 min Run Time 19.6 min Signals Test Plot Save Off 50 Hz Test Plot Save Off 50 Hz Test Plot Save Off 50 Hz Test Plot Save Off 50 Hz MS ACQUISITION PARAMETERS General Information ------- ----------- Tune File : dftpp_276.u Acquistion Mode : Scan MS Information -- ----------- Solvent Delay : 2.39 min EMV Mode : Gain Factor Gain Factor : 1.00 Resulting EM Voltage : 1753 [Scan Parameters] Low Mass : 35.0 High Mass : 550.0 Threshold : 50 Sample # : 1 A/D Samples 2 [MSZones] MS Source : 276 C maximum 350 C MS Quad : 150 C maximum 200 C END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US71226218 ----------------------------- Trace Ion Detection is OFF. EMISSION : 34.610 ENERGY : 69.922 REPELLER : 28.783 IONFOCUS : 89.208 ENTRANCE_LE : 0.000 EMVOLTS : 1670.588 Actual EMV : 1752.94 GAIN FACTOR : 1.02 AMUGAIN : 1795.000 AMUOFFSET : 123.563 FILAMENT : 1.000 DCPOLARITY : 1.000 ENTLENSOFFS : 21.835@ 3 21.835@ 50 17.318@ 69 20.831@131 22.839@219 18.322@414 21.835@502 21.835@1049 MASSGAIN : -732.000 MASSOFFSET : -40.000 END OF TUNE PARAMETERS ------------------------------------ END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------